HRID433224

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)C[C@@H](C(=O)N[C@H](C)CC(=O)O)N1C(=O)N(Cc2ccc(C=Cc3ccccc3)cc2)C(C)(C)C1=O

HCID68420215

未命名化合物

HCID178418361

未命名化合物

PRODUCTS

生成物

HCID9828091

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The compound was prepared by catalytic hydrogenation of the styryl compound obtained in Example 1 (Pd/C, 1 bar hydrogen overpressure, methanol, room temperature).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-f4c89a5c73cd4d568b801a968751f277
来源数据集: uspto-grants-2003_12
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06667334B1
来源说明: uspto-grants-2003_12

反应 SMILES

[CH3:1][C:2]1([CH3:38])[C:6](=[O:7])[N:5]([C@@H:8]([CH2:18][CH:19]([CH3:21])[CH3:20])[C:9]([NH:11][C@H:12]([CH3:17])[CH2:13][C:14]([OH:16])=[O:15])=[O:10])[C:4](=[O:22])[N:3]1[CH2:23][C:24]1[CH:29]=[CH:28][C:27]([CH:30]=[CH:31][C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)=[CH:26][CH:25]=1.[H][H]>[Pd].CO>[CH3:38][C:2]1([CH3:1])[C:6](=[O:7])[N:5]([C@@H:8]([CH2:18][CH:19]([CH3:21])[CH3:20])[C:9]([NH:11][C@H:12]([CH3:17])[CH2:13][C:14]([OH:16])=[O:15])=[O:10])[C:4](=[O:22])[N:3]1[CH2:23][C:24]1[CH:29]=[CH:28][C:27]([CH2:30][CH2:31][C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)=[CH:26][CH:25]=1