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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 433863Generated: October 29, 2026

m-Chloroperbenzoic acid → HCID 18755929, compound

https://huagongshe.com/reaction/433863

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantHCID 18755941HCID 18755941—
Solvent1,1-DichloroethaneHCID 6365—
ProductHCID 18755929HCID 18755929—

Reaction Steps

2-(2,6-Difluorophenyl)-4-[4-(2-ethylthiopyridin-5-yl)phenyl]oxazoline (Ex. No. 39; 0.60 g, 1.5 mmol) was stirred for 5 hours at 20° C. with 3-chloroperbenzoic acid (0.41 g, 1.7 mmol) in dichloroethane (10 ml). After extraction and chromatography, 2-(2,6-difluorophenyl)-4-[4-(2-ethylsulfinylpyridin-5-yl)phenyl]oxazoline was obtained, 0.21 g, colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06670307B2
Source datasetuspto-grants-2003_12
ORD IDord-5b6b77bdfd5d4404b80d138dcbba62f4
Source noteuspto-grants-2003_12