HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 72739620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 2,4-Difluoro-benzaldehyde oxime | HCID 53395027 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72739620 | HCID 72739620 | 68.4% |
Reaction Steps
In a fashion similar to that for preparation 14, 2,4-difluorobenzaldehyde oxime (2.52 g, 16.1 mmol), N-chlorosuccinimide (2.21 g, 16.5 mmol), and dimethyl formamide (25 ml) gave 2,4-difluorobenzoyl chloride oxime (2.11 g, 68%) after chromatography (silica gel, hexanes/ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06670373B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-e791cf51eb754382b6a98a2ef6fd6803 |
| Source note | uspto-grants-2003_12 |