HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 59047204, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 59047185 | HCID 59047185 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 59047204 | HCID 59047204 | 24% |
Reaction Steps
The title compound (40 mg) was prepared from compound 42A (176 mg) by procedures analogous to those described in Example 41B. mp 226-228° C. Chiral HPLC: 99% at 7.36 min (retention time) (CHIRALPAK® AD column 4.6×250 mm; 40% isopropanol in hexane over 20 minutes, 1 mL/min, monitoring at 220 nM); MS (ES): m/z 294 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06670386B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-67ca871a4f14466e8df1765d78133d79 |
| Source note | uspto-grants-2003_12 |