HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiopheneacetic acid → HCID 20493324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiopheneacetic acid | HCID 15970 | — |
| Reactant | HCID 20493318 | HCID 20493318 | — |
| Reactant | HCID 20493327 | HCID 20493327 | — |
| Product | HCID 20493324 | HCID 20493324 | — |
Reaction Steps
Hydrolyze 100 mg 1-ethoxycarbonylmethyl-3-methyleneperhydroazocin-2-one (prepared as in Example 1) with base as described in Example 3. Treat the resulting 1-carboxymethyl-3-methyleneperhydroazocin-2-one with thiolacetic acid as described in Example 3 and isolate the desired 1-carboxymethyl-3-acetylthiomethylperhydroazocin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04396616 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-f453631ae53645fda111bca21d8e22d0 |
| Source note | uspto-grants-1983_08 |