HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Benzeneethanol, alpha-methyl-, 1-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 1-Phenyl-2-propanol | HCID 94185 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Benzeneethanol, alpha-methyl-, 1-acetate | HCID 16457 | — |
Reaction Steps
Acetyl chloride (16.7 g) in dry ether (50 ml) was added dropwise to a stirred solution of 1-phenylpropan-2-ol (26.4 g) in dry ether (250 ml). The mixture was refluxed for 2 h, washed with sodium bicarbonate solution, dried (MgSO4) and evaporated to a colourless oil (27.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04396627 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-503077e2db97420c8662fa1b6b958cd4 |
| Source note | uspto-grants-1983_08 |