HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 20493842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 54114875 | HCID 54114875 | — |
| Catalyst | Dichlorocobalt hexahydrate | HCID 517166 | — |
| Product | HCID 20493842 | HCID 20493842 | — |
Reaction Steps
It is contemplated that reacting 4-benzyloxy-3-(methylsulfinyl)phenyl benzoate prepared according to the procedure of Example 3A with cobalt chloride hexahydrate and sodium bobohydride according to the procedure described in Example 1H will give 4-benzyloxy-3-(methylthio)-phenol and that substituting the latter for 4-benzyloxy-3-(methylsulfinyl)phenol in the procedures of Examples 3C and 3D will afford 1-[4-hydroxy-3-(methylthio)phenoxy]-3-[[3-(4-methoxyphenyl)-1-methylpropyl]-amino]-2-propanol (Formula I: Y=CH3S, R1 =H, ##STR16##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04396629 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-8122d8e680d1484380742daed489e10c |
| Source note | uspto-grants-1983_08 |