HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-pentanone hydrochloride → HCID 178470245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-pentanone hydrochloride | HCID 19369630 | — |
| Reactant | Ethyl imino(methylthio)acetate tetrafluoroborate | HCID 86648451 | — |
| Product | HCID 178470245 | HCID 178470245 | 60% |
Reaction Steps
The same operation as in Example (lb) was performed using 2-amino-pentan-3-one hydrochloride obtained in Example (15c) (about 10 mmol) and ethyl imino(methylthio)acetate tetrafluoroborate obtained according to a method known in the literature (J. Med. Chem., 38, 1995, 2196-2201) (about 10 mmol), to obtain 1.1 g of the title compound as a yellow solid (60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536197B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-32f6d9d3694047ab9ccad3ae945efda4 |
| Source note | uspto-grants-2013_09 |