Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-(Bromomethyl)-2-methyl-1,3-dioxolane | HCID 264604 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13175522 | HCID 13175522 | 40.1% |
Reaction Steps
Ethylamine (115 grams; 1.77 mole) and 2-methyl-2-bromomethyl-1,3-dioxolane (32 grams; 0.177 mole) were placed in a stainless steel bomb and placed on a steam bath for 5 hours. The temperature of the mixture was raised to 120° C. for 15 hours. The mixture was cooled and ether (200 ml) added to it. Sodium hydroxide (25 grams) was added and the ether layer separated and dried over magnesium sulfate. The ether was evaporated leaving the desired product (10.3 grams) as identified by nuclear magnetic resonance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04397677 |
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| Source dataset | uspto-grants-1983_08 |
|---|
| ORD ID | ord-99dc61d03dbb414486c50c48d10b71db |
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| Source note | uspto-grants-1983_08 |
|---|
