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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 434603Generated: October 27, 2026

Biphenyl → Biphenylyl phenyl iodonium tosylate

https://huagongshe.com/reaction/434603

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBiphenylHCID 7095—
ReactantHCID 178427798HCID 178427798—
SolventDiethyl EtherHCID 3283—
ProductBiphenylyl phenyl iodonium tosylateHCID 2049142463%

Reaction Conditions

Temperature135 °C

Reaction Steps

A mixture of 9.3 grams (0.023 mole) phenyliodoso tosylate and 9.25 grams (0.06 mole) biphenyl was heated to 135° C. for 1 hour and the mixture poured into 50 ml diethyl ether. After filtering off the insoluble salt and washing with ether, the product was dried. A 63% yield of biphenylyl phenyl iodonium tosylate was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04399071
Source datasetuspto-grants-1983_08
ORD IDord-b08efe69c63140588fe80863c54bad31
Source noteuspto-grants-1983_08