反应详情

温度

135 °C

A mixture of 9.3 grams (0.023 mole) phenyliodoso tosylate and 9.25 grams (0.06 mole) biphenyl was heated to 135° C. for 1 hour and the mixture poured into 50 ml diethyl ether. After filtering off the insoluble salt and washing with ether, the product was dried. A 63% yield of biphenylyl phenyl iodonium tosylate was obtained.

1. filtrationAfter filtering off the insoluble salt
2. washwashing with ether
3. customthe product was dried