Tetrahydrofuran → HCID 13092012, compound

HRID 434820Notes

Reaction equation

HRID 434820 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH:15]([OH:21])[C:16](=[NH:20])[O:17]CC)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[O:22]1CCC[CH2:23]1>C1(C)C=CC=CC=1>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH:15]1[O:21][C:23](=[O:22])[NH:17][C:16]1=[O:20])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 8028TetrahydrofuranHCID 13599058HCID 13599058, compound

Product 1

HCID 13092012HCID 13092012, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

By the procedure Method A of Example 12, ethyl 1-(2-benzyloxyphenyl)-1-hydroxymethanecarboximidate (13 g.) in 350 ml. of tetrahydrofuran was converted to toluene recrystallized 5-(2-benzyloxyphenyl)oxazolidine-2,4-dione (7.23 g., 55%; m.p. 191°-193° C.; m/e 283)

Workup

  1. customrecrystallized 5-(2-benzyloxyphenyl)oxazolidine-2,4-dione (7.23 g., 55%; m.p. 191°-193° C.; m/e 283)

Sources & evidence

ORD record
ord-78af07ebeb9a408a80fbfd2316c9040c
Source dataset
uspto-grants-1983_08
Patent number
US04399296

Reaction notes

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