HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 13092036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 13092002 | HCID 13092002 | — |
| Catalyst | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 13092036 | HCID 13092036 | — |
Reaction Steps
5-(5-Chloro-2-methoxyphenyl)oxazolidine-2,4-dione (100 mg.) was dissolved in 2.5 ml. of tetrahydrofuran. Excess acetic anhydride (4 drops) was added, and the mixture allowed to stand at room temperature for 16 hours. Evaporation to dryness gave 3-acetyl-5-(5-chloro-2-methoxyphenyl)oxazolidine-2,4-dione [Rf 0.75 (1:1 ethyl acetate: chloroform; m.p. 160°-162° C⟧
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04399296 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-5ae985892c314e77b000380124f9fc3a |
| Source note | uspto-grants-1983_08 |