HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5-Diethyl-2-(dimethoxymethyl)-1H-imidazole → 4,5-Diethyl-1H-imidazole-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5-Diethyl-2-(dimethoxymethyl)-1H-imidazole | HCID 67549747 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 4,5-Diethyl-1H-imidazole-2-carbaldehyde | HCID 86648501 | 28.5% |
Reaction Steps
The same operation as in Example (33b) was performed using 4,5-diethyl-2-(dimethoxymethyl)-1H-imidazole obtained in Example (43a) (about 8.12 mmol) and 2 N sulfuric acid (40 mL), to obtain 352 mg of the title compound as a white solid (28%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536197B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-a6150407435c4edb957c99479a1a9cfe |
| Source note | uspto-grants-2013_09 |