HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53950594, compound → HCID 54502876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53950594 | HCID 53950594 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54502876 | HCID 54502876 | 73.7% |
Reaction Steps
The compound of Example 26 (1.2 g), methylene chloride (10 ml) and pyridinium chlorochromate (1.08 g) were stirred together for 24 hours at ambient temperature. The resulting solution was filtered through a column of Fluorosil (Trade Mark) using methylene chloride as eluant. Evaporation of the solvent gave 0.87 g (73.7%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04400198 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-c13f4224df3f4d239442aad304e0fc45 |
| Source note | uspto-grants-1983_08 |