HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 20490891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 13655422 | HCID 13655422 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20490891 | HCID 20490891 | 95% |
Reaction Steps
29.5 g (0.1 mole) of 1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether were dissolved in 200 ml of chloroform and 6.4 g of 95% strength nitric acid were added. The crystallization of the salt was completed by adding 250 ml of ether. After filtering off and drying, 34 g (95% of theory) of 1-(2',4'-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-ethyl allyl ether nitrate of melting point 131° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04400388 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-3f1f9cd3f97446b3880ce6187833e492 |
| Source note | uspto-grants-1983_08 |