Hydrochloric Acid → HCID 169941, compound

Participants

Reaction Conditions

Reaction Steps

206 g (1 mole) of p-tert-octylphenol, 60 g (0.64 mole) of phenol, 121.0 g (1.49 moles) of 37% formalin and 1.5 g of 35% HCl were condensed under water reflux for 10 hours, and the reaction mixture was dehydrated by heating it to 160° C. under atmospheric pressure and then under reduced pressure to give a p-tert-octylphenol/phenol/formaldehyde co-condensate. A mixture of 60 g of zinc benzoate and 45 g of ammonium hydrogen carbonsate was added gradually over the course of 1 hour to the resulting co-condensate to give a pale yellow transparent zinc salt of the p-tert-octylphenol/phenol/formaldehyde co-condensate.

Provenance & Evidence