HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → Methyl 3-(2,6-dimethylphenyl)-carbazate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | (2,6-Dimethylphenyl)hydrazine | HCID 408103 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Methyl 3-(2,6-dimethylphenyl)-carbazate | HCID 13097166 | — |
Reaction Steps
18 g of 2,6-dimethylphenyl-hydrazine and 14 g of triethylamine were dissolved in 150 ml of ethyl ether. Keeping the temperature at 0° C., 12.5 g of methyl chloroformate were added dropwise to the solution. Precipitation of the chlorohydrate of triethylamine was observed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04401675 |
| Source dataset | uspto-grants-1983_08 |
| ORD ID | ord-d3c3ccb59f2d461fb5da495dd9b1ce52 |
| Source note | uspto-grants-1983_08 |