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HRID435441

反应详情

EQUATION

反应方程式

HRID 435441 的结构方程式

REACTANTS

反应物

3
结构：COC(=O)Cl
HCID6586

Methyl chlorocarbonate

C2H3ClO2

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：Cc1cccc(C)c1NN
HCID408103

(2,6-dimethylphenyl)hydrazine

C8H12N2

PRODUCTS

生成物

1
结构：COC(=O)NNc1c(C)cccc1C
HCID13097166

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

18 g of 2,6-dimethylphenyl-hydrazine and 14 g of triethylamine were dissolved in 150 ml of ethyl ether. Keeping the temperature at 0° C., 12.5 g of methyl chloroformate were added dropwise to the solution. Precipitation of the chlorohydrate of triethylamine was observed.

WORKUP

后处理

  1. customat 0° C.
  2. customPrecipitation of the chlorohydrate of triethylamine