HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 70638261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Methyl-1H-pyrrole-2-carbaldehyde | HCID 14504 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 70639049 | HCID 70639049 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70638261 | HCID 70638261 | 74.3% |
Reaction Steps
A mixture of 12.0 g of 1,2,3-trimethyl-1H-imidazolium iodide, 2g of potassium hydroxide and 12.0 g of N-methylpyrrole-2-carboxaldehyde in 60 ml of absolute ethanol is refluxed for 15 minutes during which time a precipitate is formed. The mixture is cooled and 10 ml of water is added. The solid is filtered off and crystallized from absolute ethanol to yield 12.3 g of the title compound, melting point 289°-291° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006137 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-25427eb0ad0246bd9e516e0820cbe1ce |
| Source note | uspto-grants-1977_02 |