HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12232349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Fluoro-6-(phenylthio)-benzyl alcohol | HCID 12232346 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12232349 | HCID 12232349 | — |
Reaction Steps
129 g of 3-fluoro-6-(phenylthio)-benzyl alcohol are dissolved in 385 ml of benzene and heated under reflux. 73 ml of thionyl chloride are added thereto and the resulting mixture is boiled for a further 30 minutes. The mixture is evaporated under reduced pressure. There is obtained 3-fluoro-6-(phenylthio)-benzyl chloride as a red-brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006145 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-db80e4db199b480a97512429479f9c64 |
| Source note | uspto-grants-1977_02 |