Sodium Methoxide → HCID 178514233, compound

Participants

Reaction Steps

A 0.6 g. portion of 1,2,4-triazole-3-carboxamide is added to 5.4 ml. of a solution of 1N sodium methoxide in methanol contained in a test tube at room temperature. The mixture is shaken vigorously. Within about 1/2 to one minute most of the solid dissolves. The mixture is quickly filtered through a sintered glass funnel with vacuum. The light yellow filtrate is allowed to stand and deposits a colorless solid. A portion of methanol is added and the solid is collected, washed with methanol and air dried for one hour yielding 0.3 g. of product.

Provenance & Evidence