HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 1-Chloro-5-methoxy-2,6-dimethylheptane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Methoxy-2,6-dimethylheptan-1-ol | HCID 21399118 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-Chloro-5-methoxy-2,6-dimethylheptane | HCID 21399083 | — |
Reaction Steps
A mixture of 3.4 g. of 1-hydroxy-5-methoxy-2,6-dimethylheptane and 3 g. of thionyl chloride and 60 ml. of dry benzene is treated with 0.2 ml. of dry dimethylformamide and then refluxed for 6 hours. After cooling, the mixture is decanted and 1-chloro-5-methoxy-2,6-dimethylheptane isolated by filtration through silica gel and distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04006188 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-7a39b80d0e5a4a259274a3e4984dbe18 |
| Source note | uspto-grants-1977_02 |