HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N'-tert-butylbenzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | tert-Butylhydrazine | HCID 81890 | — |
| Reactant | HCID 22613473 | HCID 22613473 | — |
| Solvent | Water | HCID 962 | — |
| Product | N'-tert-butylbenzohydrazide | HCID 299436 | 71% |
Reaction Steps
1-benzoyl-2tert.-butylhydrazine was prepared in 71% yield by adding benzoyl chloride to a basic solution of t-butylhydrazine in water. The procedure was the same as that for preparing 1-pivaloyl-2-tert.-butylhydrazine in Example XIX A. The product has a melting range of 94° - 95° C. and its infra-red spectrum was consistent with that of the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007165 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-76474f50e82a4fb0a6d27137e756ce6b |
| Source note | uspto-grants-1977_02 |