HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 12671198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Sec-Butylamine | HCID 24874 | — |
| Reactant | 7-chloro-6-(2-chloroethyl)-5-methyl[1,2,4]triazolo[1,5-a]pyrimidine | HCID 3638648 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12671198 | HCID 12671198 | — |
Reaction Steps
A mixture of 2.3g of 7-chloro-6-(2-chloroethyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 1g of sec-butylamine, 1.8g of sodium carbonate and 20 ml of ethanol was refluxed for 2 hours. The hot reaction mixture was then filtered and the filtrate was concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007189 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-9b201f68a2ab49968ca8a5957d493227 |
| Source note | uspto-grants-1977_02 |