HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 12671199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 7-chloro-6-(2-chloroethyl)-5-methyl[1,2,4]triazolo[1,5-a]pyrimidine | HCID 3638648 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12671199 | HCID 12671199 | — |
Reaction Steps
A mixture of 2.3g of 7-chloro-6-(2-chloroethyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 1g of isobutylamine, 1.8g of sodium carbonate and 20 ml of ethanol was treated by the same manner as described in Example 3. The crystals thus obtained were recrystallized from aqueous methanol to give 1.4g of pale yellow prisms of m.p. 143° - 145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007189 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-96bae4cf2edb4213b8309f74aeed415b |
| Source note | uspto-grants-1977_02 |