HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptylamine → HCID 12671225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptylamine | HCID 2899 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 7-chloro-6-(2-chloroethyl)-5-methyl[1,2,4]triazolo[1,5-a]pyrimidine | HCID 3638648 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12671225 | HCID 12671225 | — |
Reaction Steps
A mixture of 2g of 7-chloro-6-(2-chloroethyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 0.98g of cycloheptylamine, 3 ml of triethylamine and 20 ml of ethanol was stirred under reflux for 1.5 hours and treated thereafter as described in Example 5. The crystals thus obtained were crystallized from tetrahydrofuranisopropyl ether to give 1.4g of pale yellow needles of m.p. 197° - 198° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007189 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-fbdc9e5e3c2e41deb9a093e49b0049d8 |
| Source note | uspto-grants-1977_02 |