Tert-Butylamine → HCID 21454941, compound

Participants

Reaction Steps

A mixture of 2.6g of 7-chloro-6-(2-chlorobutyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 0.9g of tertbutylamine, 1.8g of sodium carbonate and 20 ml of ethanol was stirred at room temperature for 1 hour and then refluxed for 5 hours. The reaction mixture was thereafter treated by the same manner as described in Example 10. The crystals thus obtained were recrystallized from isopropyl alcohol-isopropyl ether to give 400 mg of pale yellow crystals of m.p. 170° C (decomp).

Provenance & Evidence