HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → 2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | 2-[6-(3,6-Dihydro-4-phenyl-1(2H)-pyridinyl)hexyl]-2,3-dihydro-3-hydroxy-1H-benz[de]isoquinolin-1-one | HCID 20364465 | — |
| Product | 2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione | HCID 16638791 | — |
Reaction Steps
Following the procedure of part (a) of example 4 but substituting 1,5-dibromopentane for the 1,6-dibromohexane, one obtains 2-(5-bromopentyl)-1H-benz[de]isoquinoline-1,3(2H)-dione; m.p. 113°-115°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007191 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-17f03022dc584da9bc4e2964e54a3f82 |
| Source note | uspto-grants-1977_02 |