HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 21454950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 3,6-Bis(5-chloro-2-piperidyl)-2,5-piperazinedione | HCID 114728 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21454950 | HCID 21454950 | — |
Reaction Steps
One mole of 3,6-bis(5-chloro-2piperidinyl)-2,5-piperazinedione is stirred in 150 parts of acetone and 2.2 moles of benzyl bromide is added. The mixture is stirred 24 hours and refluxed 24 hours. The solvent is removed in vacuo and treated as in the preparation of 3,6-bis-(1-methyl-5-chloro-2-piperidinyl)-2,5-piperazinedone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007190 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-2b990c78f42043cba73466e3eaceff3c |
| Source note | uspto-grants-1977_02 |