HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Thiophenecarboxylic acid, tetrahydro-4-oxo-, methyl ester → HCID 612691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Thiophenecarboxylic acid, tetrahydro-4-oxo-, methyl ester | HCID 98424 | — |
| Reactant | 4-Fluorobenzene-1,2-diamine | HCID 164584 | — |
| Product | HCID 612691 | HCID 612691 | — |
Reaction Steps
In a similar fashion 4-fluoro-o-phenylenediamine is condensed with methyl tetrahydro-4-oxo-3-thiophenecarboxylate to give a mixture of 7-fluoro- and 6-fluoro-1,3,4,9-tetrahydro-10H-thieno[3,4-b][1,5]benzodiazepin-10-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04007272 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-5b85e2b5ff1d4b7c936ad68483496796 |
| Source note | uspto-grants-1977_02 |