huagongshe.com
HRID436251

反应详情

EQUATION

反应方程式

HRID 436251 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)OCc1ccccc1
HCID10387

Benzyl chloroformate

C8H7ClO2

结构：CCC[C@@H](N)C(=O)O
HCID439575

(2R)-2-Aminopentanoic acid

C5H11NO2

PRODUCTS

生成物

1
结构：CCC[C@@H](NC(=O)OCc1ccccc1)C(=O)O
HCID10106192

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Na+].[OH-]
溶剂HCID14798

Sodium Hydroxide

HNaO

PROCEDURE

实验过程

In the routine manner, H-D-Nva-OH is reacted with carbobenzoxy chloride in 2 N sodium hydroxide and the resultant compound is recrystallized from ethyl acetatepetroleum benzine. The procedure gives needles melting at 83°-84° C.

WORKUP

后处理

  1. customthe resultant compound is recrystallized from ethyl acetatepetroleum benzine