Diethylamine → HCID 131710655, compound

HRID 436317Notes

Reaction equation

HRID 436317 reaction equation
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].[Cl:6][CH:7]([C:11]1[CH:16]=[CH:15][C:14]([CH:17]2[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]2)=[C:13]([Cl:23])[CH:12]=1)[C:8]([OH:10])=[O:9]>CCCCCC>[CH2:1]([NH2+:3][CH2:4][CH3:5])[CH3:2].[Cl:6][CH:7]([C:11]1[CH:16]=[CH:15][C:14]([CH:17]2[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]2)=[C:13]([Cl:23])[CH:12]=1)[C:8]([O-:10])=[O:9]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 37494Fenclorac

Product 1

HCID 131710655HCID 131710655, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Anhydrous diethylamine (0.11 moles) is added dropwise to a stirred solution of α,3-dichloro-4-cyclohexylphenylacetic acid (0.10 moles) in 100 ml. of n-hexane at 0° C. The precipitate is collected on a filter, washed with n-hexane, and dried in a vacuum desiccator to obtain α,3-dichloro-4-cyclohexylphenylacetic acid, diethylammonium salt.

Workup

  1. customat 0° C
  2. customThe precipitate is collected on a filter
  3. washwashed with n-hexane
  4. customdried in a vacuum desiccator

Sources & evidence

ORD record
ord-94255b49c3144dd690f44f376fc4dabc
Source dataset
uspto-grants-1977_02
Patent number
US04008269

Reaction notes

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