HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21454470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-naphthalen-1-yl-3-(pyridin-4-ylmethyl)urea | HCID 915038 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21454470 | HCID 21454470 | — |
Reaction Steps
A solution of 2.77 gm. (0.01 mole) of 1-(1-naphthyl)-3-(4-pyridylmethyl)urea and 50 ml. of chloroform is saturated with anhydrous hydrogen chloride. The solution is then evaporated to dryness in vacuo. The residue is crystallized from alcohol Skellysolve B (9:1 v/v) to give 1-(1-naphthyl)-3-(4-pyridylmethyl)urea hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04008326 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-96be6f5ff3d54d1ab89852d29dec29f0 |
| Source note | uspto-grants-1977_02 |