HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinium chloride → HCID 12349082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinium chloride | HCID 115031 | — |
| Reactant | 1-Ethoxy-3-methyl-3,4-dihydroisoquinoline | HCID 12349040 | — |
| Product | HCID 12349082 | HCID 12349082 | — |
Reaction Steps
In a manner similar to that of Step B of Example 1, condensation of 1-ethoxy-3-methyl-3,4-dihydroisoquinoline (1.0 g.) and hydrazine monohydrochloride (0.36 g.) and three recrystallizations of the resulting product from ethanol-ether afforded 1-hydrazino-3-methyl-3,4-dihydroisoquinoline (V: Y=CH3, Y'= Z=Z'=H) hydrochloride (m.p. 174°-176° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009170 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-f4c5362be3f945a0ac1672464c83059b |
| Source note | uspto-grants-1977_02 |