참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chloroethanol | HCID 34 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 1-Propanesulfonyl chloride, 2-methyl- | HCID 182236 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 2-Chloroethyl 2-methylpropane-1-sulfonate | HCID 22769942 | — |
반응 단계
A mixture was formed containing 6.7 ml. of ethylene chlorohydrin, 70 ml. of ether and 15.6 g. of isobutane sulfonyl chloride. Then, 14 ml. of triethylamine was added dropwise to the mixture with stirring in an ice bath over a period of 30 minutes at 12°-14° C. While stirring the mixture was allowed to warm to 23° C. (1 hour) and was then washed with water (100 ml.), dried over magnesium sulfate and evaporated to yield 19.7 g. of a colorless oil. nD30 1.4502.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04009191 |
|---|
| 출처 데이터셋 | uspto-grants-1977_02 |
|---|
| ORD ID | ord-33eaffd9f0cf4cea8556ffd18930db3e |
|---|
| 출처 메모 | uspto-grants-1977_02 |
|---|
