HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 8-(2-furyl)octanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 11790484 | HCID 11790484 | — |
| Product | Methyl 8-(2-furyl)octanoate | HCID 557175 | — |
Reaction Steps
19 g of 8-(2-furyl)-octanoic acid were refluxed for 4 hours with 100 ml of methanol and 1.5 ml of sulphuric acid. The mixture was then evaporated to one third of its original volume. 100 g. of ice-water were then added, whereupon the mixture was extracted with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009187 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-4bd25e49329e411fa22a71789ea2e754 |
| Source note | uspto-grants-1977_02 |