反应详情

19.4g (0.1 mole) of 4-acetamino-3-methyl-nitrobenzene, 30g of dimethylformamide and 1g of fresh-developed Raney nickel were fed in an autoclave, 50kg/cm2 of hydrogen was then fed thereto, and, after the reaction was carried out at 60° to 120° C while stirring, the reaction mixture was removed immediately, the Raney nickel was removed while hot, and thereafter the product was poured into 100ml of methanol to separate the 4-acetamino-3-methylaniline produced.

1. customwas carried out at 60° to 120° C
2. customthe reaction mixture was removed immediately
3. customthe Raney nickel was removed while hot, and thereafter the product
4. additionwas poured into 100ml of methanol
5. customto separate the 4-acetamino-3-methylaniline
6. customproduced