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HRID436546

反应详情

EQUATION

反应方程式

HRID 436546 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccc(S(=O)(=O)Cl)cc1
HCID7397

p-Toluenesulfonyl chloride

C7H7ClO2S

结构：Cc1cc([N+](=O)[O-])ccc1N
HCID7441

2-Methyl-4-nitroaniline

C7H8N2O2

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)Nc2ccc([N+](=O)[O-])cc2C)cc1
HCID4430080

Benzenesulfonamide, 4-methyl-N-(2-methyl-4-nitrophenyl)-

C14H14N2O4S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

152g (1 mole) of 4-amino-3-methyl-nitrobenzene, 80g of sodium carbonate and 500g of water are mixed, 230g (1.2 moles) of p-toluenesulfonyl chloride were added thereto while stirring, and the reaction was carried out for 3 hours at 70° C to obtain 290g of 4-(N-p-toluenesulfonyl)amino-3-methylnitrobenzene.