Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → N,N'-Heptamethylenebis(4-pentyloxybenzamide)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 1,7-Heptanediamine | HCID 69533 | — |
| 반응물 | p-Pentoxybenzoyl chloride | HCID 94910 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | N,N'-Heptamethylenebis(4-pentyloxybenzamide) | HCID 21453005 | — |
반응 단계
m.p. 155°-156° C., 29.9 g., was prepared as in Example 1 using 50 g. of 4-pentyloxybenzoyl chloride in 200 ml. of ethylene dichloride, 13.0 g. of 1,7-heptanediamine, 250 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009208 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-237b5978bc3f4f54b0c9a58e51765442 |
| 출처 메모 | uspto-grants-1977_02 |