HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 4200952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 1,3-Benzodioxole-5-carbonyl chloride | HCID 2734749 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 4200952 | HCID 4200952 | — |
Reaction Steps
m.p. 183°-185° C., 19.4 g., was prepared as in Example 1 using 3,4-methylenedioxybenzoyl chloride (from 30 g. of 3,4-methylenedioxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 9.3 g. of 1,6-hexanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol using decolorizing charcoal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-05cf657e113d4178955300031f45271a |
| Source note | uspto-grants-1977_02 |