HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 21453014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,7-Heptanediamine | HCID 69533 | — |
| Reactant | 4-(2-Chloro-1,1,2-trifluoroethoxy)benzoyl chloride | HCID 21452880 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 21453014 | HCID 21453014 | — |
Reaction Steps
m.p. 153°-154° C., 16.0 g., was prepared as in Example 16 using 4-(2-chloro-1,1,2-trifluoroethoxy)benzoyl chloride (from 23.0 g. of the corresponding acid as in Example 16) in 150 ml. of ethylene dichloride, 5.8 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-10c26637b96e40219c9efffbde17d349 |
| Source note | uspto-grants-1977_02 |