HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 53740612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hept-3-ene-1,7-diamine | HCID 53866113 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53740612 | HCID 53740612 | — |
Reaction Steps
m.p. 141°-143° C., 10.2 g., was prepared as in Example 21 using 8.37 g. of 3-heptene-1,7-diamine, 50 ml. of ethylene dichloride, 18.0 g. of potassium carbonate, 100 ml. of water, 22.4 g. of 4-methoxybenzoyl chloride in 50 ml. ethylene dichloride and recrystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-37cddb9afff44fe0866106b8d0f35054 |
| Source note | uspto-grants-1977_02 |