HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cadaverine → HCID 21452954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cadaverine | HCID 273 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 21452954 | HCID 21452954 | — |
Reaction Steps
m.p. 154°-155° C., 13.8 g., was prepared as in Example 1 using 24.6 g. of 4-trifluoromethoxybenzoyl chloride in 200 ml. of ethylene dichloride, 5.1 g. of 1,5-pentanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 300 ml. ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-1ac22d4ef1444b20a861c302ceeb4e29 |
| Source note | uspto-grants-1977_02 |