HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanone, 1-bromo-3-chloro- → HCID 53993791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanone, 1-bromo-3-chloro- | HCID 148646 | — |
| Reactant | HCID 12612400 | HCID 12612400 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53993791 | HCID 53993791 | — |
Reaction Steps
In the manner given in Example 1, 7-bromo-2-hydrazino-5-(2-pyridyl)-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 1 -bromo-3-chloro-propanone under nitrogen to give 7-bromo-2-[[2-bromo-1-(chloromethyl)ethylidene]hydrazino]-5-(2-pyridyl)-3H-1,4-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028356 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-6ec41391ad3d48e88f216bd01ceb8c5a |
| Source note | uspto-grants-1977_06 |