HRID436790

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID90494

1-Hydroxy-3-chloroacetone

C3H5ClO2

结构：NNC1=Nc2ccc([N+](=O)[O-])cc2C(c2ccccc2)=NC1

HCID22768399

未命名化合物

PRODUCTS

生成物

结构：O=[N+]([O-])c1ccc2c(c1)C(c1ccccc1)=NCC(NN=C(CO)CCl)=N2

HCID86734824

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

In the manner given in Example 1, 7-nitro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 1-chloro-3-hydroxypropanone under nitrogen to give 7-nitro-2[[2-chloro-1-(hydroxymethyl)ethylidene]hydrazino]-5-phenyl-3H-1,4-benzodiazepine.