HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-2-hydrazinyl-5-phenyl-3H-1,4-benzodiazepine → HCID 86734826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-2-hydrazinyl-5-phenyl-3H-1,4-benzodiazepine | HCID 12390874 | — |
| Reactant | HCID 21431482 | HCID 21431482 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86734826 | HCID 86734826 | — |
Reaction Steps
In the manner given in Example 1, 7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 5-carbomethoxy-2-oxopentyl methanesulfonate under nitrogen to give 7-chloro-2-[[2-hydroxy-1-(3-carbomethoxypropyl)ethylidene]hydrazino] -5-phenyl-3H-1,4-benzodiazepine, methanesulfonate ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028356 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-a00466b43a8949c28aaf8691ab6cd2f3 |
| Source note | uspto-grants-1977_06 |