HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-chloro-2-hydrazino-5-(2,6-difluorophenyl)-3H-1,4-benzodiazepine → HCID 53868323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-chloro-2-hydrazino-5-(2,6-difluorophenyl)-3H-1,4-benzodiazepine | HCID 20291823 | — |
| Reactant | HCID 20824368 | HCID 20824368 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53868323 | HCID 53868323 | — |
Reaction Steps
In the manner given in Example 1, 7-chloro-2-hydrazino-5-(2,6-difluorophenyl)-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 1-chloro-6-hydroxy-2-hexanone under nitrogen to give 7-chloro-2-[[2-chloro-1-(4-hydroxybutyl)ethylidene]hydrazino]-5-(2,6-difluoropheny1)-3H-1,4-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028356 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-1822dd97edd44829b462ade95631f5d0 |
| Source note | uspto-grants-1977_06 |