HRID436883

反应详情

EQUATION

反应方程式

HRID 436883 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Further, 0.5 ml of quinoline and 20 g of 0.25% Pd-Lindlar catalyst was added in a solution of 1,280 g of the said dehydronerolidol in 2,000 ml of n-hexane and the mixture was hydrogenated at room temperature and normal pressure. After post-treatment, the reaction mixture was subjected to vacuum distillation to give 1,170 g of nerolidol having b.p. 105° - 110° C. (0.5 mmHg).

WORKUP

后处理

  1. customwas hydrogenated at room temperature
  2. distillationAfter post-treatment, the reaction mixture was subjected to vacuum distillation