HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 85857780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86733072 | HCID 86733072 | — |
| Product | HCID 85857780 | HCID 85857780 | — |
Reaction Steps
The starting material is obtained as follows: The solution of 10 g of 3-chloro-2'-fluoro-6-phenylmercaptomethyl-benzophenone ethylene ketal (Example 2) in 50 ml of methyl iodide is refluxed under nitrogen for 5 days. It is evaporated and the formed methyl phenyl thioether distilled off at 60°/0.1 mm Hg, to yield the 3-chloro-2'-fluoro-6-iodomethyl-benzophenone ethylene ketal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028381 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-ae71c85eaa9b4709a3b64cab8c8416e0 |
| Source note | uspto-grants-1977_06 |